Abstract The reliable determination of materials' mechanical properties is a fundamental factor for their application in engineering, and the estimation of the measurement uncertainty in testing laboratories has a direct impact on the interpretation of the results. Recent literature demonstrates that one of the most widely used methodologies for uncertainty estimation, the Guide to the Expression of Uncertainty in Measurement (GUM), has limitations, especially in cases where the mathematical model has a high degree of non-linearity. Furthermore, it makes approximations for the final probability distribution. In these cases, it is recommended that the measurement uncertainty is determined by the Monte Carlo Method (MCM), which considers the propagation of the distribution rather than the propagation of uncertainties. Thus, given the limitations of the GUM method and the importance of estimating the measurement uncertainty of mechanical tests, this work aims to implement the measurement uncertainty estimation for the plane-strain fracture toughness (KIC) test of metallic materials through the Monte Carlo Method. The results of the work confirm the importance of estimating the measurement uncertainty of fracture toughness tests.

Abstract The evaluation of material fracture mechanic properties has had an increasing need, especially in the oil and gas industries. This scenario requires quality assurance of fracture toughness tests. This article describes the activities carried out when implementing the Quality Management System (QMS) for the fracture toughness tests at the Physical Metallurgy Laboratory (LAMEF) in the Federal University of Rio Grande do Sul (UFRGS), Brazil, in order to achieve the management and technical requirements of ISO/IEC 17025. Since LAMEF was previously accredited in performing other tests, most of the adequacy was related to the technical requirements of the ISO/IEC 17025 standard. After performing the required adjustments and after an external audit, the Brazilian Institute of Metrology, Quality and Technology (Inmetro) accredited LAMEF to the fracture toughness tests. The accreditation of these tests is unprecedented in Brazil, and we expect this work to encourage other Brazilian and world laboratories to seek the implementation and accreditation of QMS for fracture mechanics tests.